专利摘要:
1473105 Ketone solutions of mixed herbicides LILLY INDUSTRIES Ltd 8 Aug 1974 [10 Aug 1973] 37945/73 Heading A5E A stable liquid herbicidal composition comprises a dinitroaniline herbicide and a N-aryl- N'-alkoxy urea herbicide dissolved in a non- phytotoxic alicyclic ketone, the ratio of dinitroaniline to urea being from 4:1 to 1:4. Optional ingredients are other solvents and non-ionic or anionic emulsifiers containing no free alcohol or polyalcohol. Typical composition ingredients are N, N-dipropyl-4-trifluoromethyl-2, 6-dinitroaniline, N-ethyl-N-2-methylallyl-4-trifluoromethyl-2, 6-dinitroaniline, N. N- dipropyl-4-sulphamoyl-2, 6-dinitroaniline: N-(3, 4-dichlorophenyl)-N'-methyl-N'-methoxy urea; and cyclohexanone or 3, 5, 5-trimethylcyclohex-2-en-1-one. The compositions may be diluted with water and used for combating weeds in crops.
公开号:SU1243606A3
申请号:SU742054979
申请日:1974-08-09
公开日:1986-07-07
发明作者:Лидл Рой
申请人:Лилли Индастриз Лимитед (Фирма);
IPC主号:
专利说明:

This invention relates to a plant protection agent, thermoglobin {, namely, a stable herbicidal emulsifiable concentrate based on a mixture. two active herbicides.
 The aim of the invention is to increase stability.
The concentrate is obtained by dissolving the required amounts of N, N-dipropyl-4-trifluoromethyl-2,6-dinitroaniline (trifthuralin) and N- (3, i dichlorophenyl) -N-methyl-N-methoxy-chevine (3,5,5,5 linuron) trimethylcyclohex 2-en-1-one and with a large amount of aromatic solvent ao-chlorotoluene. The solution is filtered and emulsified, having previously checked that the emulsifier does not contain free alcohol, with stirring. Then the rest of the aromatic is poured
Trifluralin, .100% Linuron, 100% Agent stefan 603-1 Agent stefan 603-2 Acetone
Dimethylformamide dimethyl sulfoxide
To simulate industrial use, small amounts of each emulsifiable concentrate are added to a large volume of water (1 g to 100 ml) and the diluted emulsions are mixed in an apparatus designed to mix the solutions in bottles by rotating in
any solvent, the solution is filtered, it is packaged.
Example 1. The study of the stability of the concentrate.
The composition of the emulsifiable concentrate (EAF-190), g / l:
Trifluralin, 100% 240 Linuron, 100% 120
Calcium dodecylbenzene-sulfonate50
Nonylphenylethoxylate 50 (agent stefan 603-1) 3 "5.5-Trimethyl-cyclohex-2-ene-he
(isophorone) 150
o-chlorotoludo 1 l
For comparison, the following emulsifiable concentrates are used. one.
Table 1
240 120 50 50
up to 1 l
up to 1 l
for several hours. Next, the resulting emulsions are examined, photographed, and filtered through a Büchner funnel using a Whatman No. 1 paper filter. The paper filters are dried, re-photographed, and weighed. The data obtained are presented in Table. 2
The composition
Acetone Based
Based on dimethylformamide
Based on dimethyl sulfoxide
EAF
Example 2. Conducted a test - two months after treatment
The randomly selected percentage counts of four repetitions and 25 weeds were compared to untreated winter crops in neither of the randomly selected sites.
EAF-190 herbicide to Prevention Occurrence Percentage of debris treated
Dov. The consumption of the composition was ekkultur compared with untreated 4 l / ha, these are shown in Table. 3
Table 3
Experiment Percentage of debris compared to untreated culture
10.9
22,8
32.6
 G5
Before use concentrate solids and not observed
kept for a long time with the purpose of pro-bleaching, checking its stability. For example, 45
after 6 months storage at temperature. Thus, the proposed Herr 4, 25, and 37 C do not observe any biobicidal emulsifiable concentrate.
decrease in stability, do not form; possesses high stability.

Compiled by N. Kibalova Editor L. Gratilo Tehred L. Oleinik. Proofreader And, Muska
Order 3720/59 - Circulation 679 Subscription
VNIIPI USSR State Committee
for inventions and discoveries 113035, Moscow, Zh-35, Raushsk nab., d, 4/5
Production and printing company, Uzhgorod, st. Project, 4
table 2

Weight of crystals B, g
Dol B from A,%
 .

37.5 25.6
27.3 0.7
权利要求:
Claims (1)
[1]
. STABLE HERBICIDE EMULTIABLE CONCENTRATE, including N, C-dipropyl-4-trifluoromethyl ~ 2,6-dinitroaniline and I- (3,4-dichlorophenyl ~ -H-methyl-I-methoxyurea in a ratio of 2: 1, emulsifier and solvent, o The result is that, in order to increase stability, it contains 3,5,5-trimethylcyclohex-2 ~ en ~ 1-one, as an emulsifier - a mixture of calcium dodecylbenzenesulfonate and nonylphenylethoxylate in the ratio 1: 1, and as a solvent'-o-chlorotoluene in the following ratio of components, g / l: Mixture * · 360
Specified Emulsifier 100. 3,5,5-trimethylcyclohex-2-en-1-one 150 o-chlorotoluene
The rest is up to 1 l £
N, Ν-dipropyl-4-trifluoromethyl-2,6-dinitroaniline and N- (3,4-dichloro phenyl) -I ^ methyl-I-methoxyurea in a 2: 1 ratio.
and . SU ... 1243606 AZ
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同族专利:
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引用文献:
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US3373010A|1964-10-08|1968-03-12|Du Pont|Herbicidal composition and method|
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CH533421A|1970-02-02|1973-02-15|Ciba Geigy Ag|Biocidal agent|
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IL36220D0|1970-02-27|1971-04-28|Ciba Geigy Ag|Use of a phenylurea for combating weeds in wheat,oats,rye,barley,rice and cotton|
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DE2037265A1|1970-07-28|1972-02-03|Badische Anilin & Soda Fabrik AG, 6700 Ludwigshafen|herbicide|
DE2039042A1|1970-08-06|1972-02-17|Hoechst Ag|Herbicides|
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CA985523A|1971-06-30|1976-03-16|American Cyanamid Company|Inhibiting plant bud growth|DE2534042A1|1975-07-30|1977-02-17|Shell Int Research|HERBICIDE MEDIUM|
IT1131750B|1980-06-06|1986-06-25|Montedison Spa|STABLE FORMULATIONS OF N--N'METOXY-N'-METHYLENEAND 2,6-DINITOR-N, N-DIPROPYL-4-TRIFLUOR METHYLANILINEIN EMULSION|
CH652888A5|1982-08-25|1985-12-13|Sintagro Sa|STABLE, LIQUID PREPARATION WITH HERBICIDAL EFFECT AND METHOD FOR THE PRODUCTION THEREOF.|
IL116147A|1994-11-30|2002-05-23|Aventis Cropscience Sa|Emulsifiable composition for the control of insects|
IL116148A|1994-11-30|2001-03-19|Rhone Poulenc Agrochimie|Emulsifiable composition for the control of insects|
MA40840A|2014-10-22|2017-08-29|Ishihara Sangyo Kaisha|HERBICIDE COMPOSITION|
法律状态:
优先权:
申请号 | 申请日 | 专利标题
GB3794573A|GB1473105A|1973-08-10|1973-08-10|
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